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Reaction Calorimeter

The RC HP-1000AE simulates factory batch or semi-batch chemical reactions on a liter scale under laboratory conditions. It measures real-time exothermic heat flow in the reactor to obtain thermal behavior data, including total and specific exothermic heat, real-time thermal conversion rate, and material accumulation. It calculates adiabatic temperature rise and maximum temperature after reaction runaway (MTSR). This data is used to assess reaction runaway severity and process hazard level, providing a basis for optimizing and scaling up the target reaction.


Test Parameters

Reaction Heat Release, Specific Heat of Reaction, Maximum Temperature of Runaway System


Applicable Fields

Fine Chemicals

Features1

Features

Specifications

Specifications

Applications

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Features

Specifications

Calorimetric Methods Heat Flow, Power Compensation (Optional), Reflux (Optional)
Temperature Control
Vessel Temperature Range  -25–200 °C
Oil Bath Temperature Range -45–250 °C
Control Modes Isothermal, Constant Temperature, Scanning
Temperature Resolution 1.0 mK
Sample Temperature Control Precision ± 0.1 K
Silicone Oil Circulation Rate -35–76 L/min
Power Control
Driver Voltage Range 0–50 VDC
Maximum Driver Current 3.0 A
Maximum Heater Power 120 W
Atmospheric Pressure Glass Reactor (Optional)
Reactor Volume 1000 mL, other volumes available upon request
Working Pressure Atmospheric Pressure
Reactor Material Glass
Medium-Pressure Glass Reactor (Optional)
Reactor Volume 1000 mL, other volumes available upon request
Working Pressure 0.6 MPa or 1.2 MPa
Reactor Body Material Glass
Reactor Lid Material 316L Stainless Steel or Hastelloy
High-Pressure Metal Reactor (Optional)
Reactor Volume 1000 mL, other volumes available upon request
Working Pressure 10 MPa
Reactor Body Material 316L Stainless Steel or Hastelloy
Agitator
Maximum Speed 2000 r/min, optional 3000 r/min
Maximum Torque 75 N·cm, optional 300 N·cm
Agitator Type Anchor or Blade
Agitator Material PTFE, 316L, or Hastelloy
Injection System
Injection Channels 1 liquid injection, 1 solid injection port, 1 gas injection port; expandable to 4
Precision Balance Capacity 3100 g, accuracy 0.01 g
Injection Pumps Medium-Pressure Pump: Electromagnetic diaphragm pump, maximum flow rate 2 L/h
High-Pressure Pump: Precision plunger pump, maximum flow rate 2.4 L/h
Other Parameters
Power Supply 3*400V/50Hz (±10%)/20A
Power 7000 VA
Test Area Dimensions 1200 mm × 600 mm × 1850 mm
Oil Bath Dimensions 600 mm × 700 mm × 1300 mm
Oil Bath Weight 210 kg
otal Machine Weight 300 kg

 

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